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Engineering of Organic Nanocrystals ...

Kilani, Mohamed.

Engineering of Organic Nanocrystals by Electrocrystallization.

Record Type:	Electronic resources : Monograph/item
Title/Author:	Engineering of Organic Nanocrystals by Electrocrystallization.
Author:	Kilani, Mohamed.
Published:	Ann Arbor : ProQuest Dissertations & Theses, 2017
Description:	80 p.
Notes:	Source: Masters Abstracts International, Volume: 56-04.
Notes:	Adviser: Guangzhao Mao.
Contained By:	Masters Abstracts International56-04(E).
Subject:	Materials science.
Online resource:	http://pqdd.sinica.edu.tw/twdaoapp/servlet/advanced?query=10280712
ISBN:	9781369824759

Engineering of Organic Nanocrystals by Electrocrystallization.
Kilani, Mohamed.

Engineering of Organic Nanocrystals by Electrocrystallization. - Ann Arbor : ProQuest Dissertations & Theses, 2017 - 80 p.

Source: Masters Abstracts International, Volume: 56-04.

Thesis (M.S.)--Wayne State University, 2017.

This work discusses the experimental and theoretical methods used to control the morphology of nanocrystals. The hypothesis of the thermodynamic/kinetic control of the morphology was verified. We applied the electrocrystallization to make K(def)TCP nanocrystals and we tuned the electrochemical parameters to determine their influence on the nanocrystals morphologies. The characterization was mainly performed with AFM and FE-SEM. We presented in this work the possibility to control the morphology of K(def)TCP using the electrochemical parameters. The obtained shapes ranged from nanorods to rhombohedral shape, which is reported for the first time. The observed growth behavior was modeled and simulated with a method based on Monte-Carlo techniques. The simulation results show a qualitative match with the experimental findings. This work contributes to the understanding of the crystal growth behavior and the thermodynamic/kinetic morphology transition using electrocrystallization.

ISBN: 9781369824759Subjects--Topical Terms:

221779
Materials science.

Engineering of Organic Nanocrystals by Electrocrystallization.
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500 $a Source: Masters Abstracts International, Volume: 56-04.
500 $a Adviser: Guangzhao Mao.
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520 $a This work discusses the experimental and theoretical methods used to control the morphology of nanocrystals. The hypothesis of the thermodynamic/kinetic control of the morphology was verified. We applied the electrocrystallization to make K(def)TCP nanocrystals and we tuned the electrochemical parameters to determine their influence on the nanocrystals morphologies. The characterization was mainly performed with AFM and FE-SEM. We presented in this work the possibility to control the morphology of K(def)TCP using the electrochemical parameters. The obtained shapes ranged from nanorods to rhombohedral shape, which is reported for the first time. The observed growth behavior was modeled and simulated with a method based on Monte-Carlo techniques. The simulation results show a qualitative match with the experimental findings. This work contributes to the understanding of the crystal growth behavior and the thermodynamic/kinetic morphology transition using electrocrystallization.
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